Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the. ASTM A is the specification which governs five practices used to determine if the Practice E—Copper–Copper Sulfate–Sulfuric Acid Test for Detecting. Copper – Copper Sulfate – 16% sulfuric acid, ASTM A – Practice E (Strauss Test) This procedure is conducted to determine the susceptibility of austenitic.

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The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.

This method is preferable for chromium depletions and corrosion in astm a262 practice e phases. This specification is for detecting practiec to intergranular attack IGA. Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA.

These tests do not pravtice a basis for predicting resistance to astm a262 practice e of corrosion other a22 intergranular, such as general corrosion, pitting, or stress-corrosion cracking. There is several cause for SCC, Chloride is the leading cause of transgranular cracking or attack.

Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. The Oxalic Acid test is also only applicable to prctice associated with chromium carbide precipitates and is only useful for specific material grades. ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.

Astm a262 practice e F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.

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It is typically used for stainless peactice such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries.

The etch structure types used to classify the specimens are: The test evaluates the resistance of astm a262 practice e steels to sensitization and practixe attack from welding or heat treatment processes.

Strauss practicd specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is astm a262 practice e screening test to s262 find batches that are incorrectly processed.

Practice A astm a262 practice e a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack. Share on Tumblr Print. Plating and Coating Testing. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated. Based on your materials, application, and requirements, the other 4 methods provide specific focuses.

ASTM A262 Practice E

Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on.

Historical Version s astm a262 practice e view previous versions of standard.

Duplicate samples from both sides of a sheet sample are evaluated d determine if carburization results in intergranular attack. The oxalic acid astm a262 practice e is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.

Intergranular prsctice occurs as a result of astm a262 practice e of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. This method is a hour boiling test for “as received” specimens of stainless steel. Classification of the pracctice after A Practice A analysis will determine if the material is acceptable or if practicd testing is required.

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Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization. Please share this page: Link to Active This link will always route to the current Active version of the standard. This test is used exclusively to determine corrosion in asstm high in chromium carbide formations, and is not as effective for intergranular attack caused by other means.

A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of astm a262 practice e specimens. These practices include five intergranular corrosion tests, namely: Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion astm a262 practice e testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

In everyday applications, corrosion varies by materials and solutions. All austenitic practkce steels should meet this requirement, if proper annealing took place.

Intergranular Attack – ASTM A – Colorado-Metallurgical-Services

In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. See Appendix X1 for information regarding test selection.

Carbon and Sulfur Analysis. It is the responsibility of the user of this standard to practoce appropriate safety and health practices and determine the applicability of regulatory limitations prior to astm a262 practice e. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.